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Leila, Djahnit, Mar, López-González, Fatima, Belhadj, Abddelyamine, Naitbouda, Ali, Benosmane, Nacereddine, Haddaoui. (1397). Effect of polyethylene glycol and propyltrimethoxysilane on structural and optical properties of zinc oxide nanoparticles synthesized by sol–gel process. , 12(3), 159-167. doi: 10.1007/s40094-018-0303-2
Djahnit Leila; López-González Mar; Belhadj Fatima; Naitbouda Abddelyamine; Benosmane Ali; Haddaoui Nacereddine. "Effect of polyethylene glycol and propyltrimethoxysilane on structural and optical properties of zinc oxide nanoparticles synthesized by sol–gel process". , 12, 3, 1397, 159-167. doi: 10.1007/s40094-018-0303-2
Leila, Djahnit, Mar, López-González, Fatima, Belhadj, Abddelyamine, Naitbouda, Ali, Benosmane, Nacereddine, Haddaoui. (1397). 'Effect of polyethylene glycol and propyltrimethoxysilane on structural and optical properties of zinc oxide nanoparticles synthesized by sol–gel process', , 12(3), pp. 159-167. doi: 10.1007/s40094-018-0303-2
Leila, Djahnit, Mar, López-González, Fatima, Belhadj, Abddelyamine, Naitbouda, Ali, Benosmane, Nacereddine, Haddaoui. Effect of polyethylene glycol and propyltrimethoxysilane on structural and optical properties of zinc oxide nanoparticles synthesized by sol–gel process. , 1397; 12(3): 159-167. doi: 10.1007/s40094-018-0303-2

Effect of polyethylene glycol and propyltrimethoxysilane on structural and optical properties of zinc oxide nanoparticles synthesized by sol–gel process

Journal of Theoretical and Applied Physics
مقاله 1، دوره 12، شماره 3، آذر 2018، صفحه 159-167  XML اصل مقاله (723.5 K)
شناسه دیجیتال (DOI): 10.1007/s40094-018-0303-2
نویسندگان
Djahnit Leila email 1؛ López-González Mar2؛ Belhadj Fatima3؛ Naitbouda Abddelyamine4؛ Benosmane Ali5؛ Haddaoui Nacereddine6
1Laboratoire de Physico-Chimie des Hauts Polymères, Université de Ferhat Abbes, Sétif-1;Département de Chimie, Université de Hassiba Benbouali
2Instituto de Ciencia y Tecnología de Polímeros (ICTP-CSIC)
3Département de Chimie, Université de Hassiba Benbouali;Chemical Materials Laboratory, University Ahmed Benballa
4Centre de Développement des Technologies Avancées
5Département de Chimie, Université de Hassiba Benbouali;Laboratory of Molecular Chemistry, Environmental Control and Physico-Chemical Measurements, University of Mentouri
6Laboratoire de Physico-Chimie des Hauts Polymères, Université de Ferhat Abbes, Sétif-1
چکیده
AbstractZinc oxide nanoparticles (ZnO NPs) are prepared by sol–gel process, using both polyethylene glycol (PEG-400) as surfactant and propyltrimethoxysilane (PTMS) as capping agent. Surface modification is performed in situ procedure. The physical parameters such as strain and stress values are calculated via the Williamson–Hall plot (W&H) assuming a uniform deformation model (UDM) and uniform stress deformation model, and by the size and strain plot method (SSP). The results show that the crystallite size estimated from Scherrer’s formula, (W&H), (UDM), (SSP) and the particle size estimated from DSL are inter-correlated, which confirm the small size and the isotropic nature of our ZnO NPs. The FTIR spectroscopy illustrates that PEG-400 and PTMS could be adsorbed at the ZnO NPs surface. The distinct emission peak in the blue band is located at 490 nm and E2 (high) mode is situated at 436 cm−1. Both results confirm the oxygen deficiency in the ZnO NPs.
کلیدواژه‌ها
Sol–gel synthesis؛ Zinc Oxide؛ PEG؛ 400؛ Propyltrimethoxysilane؛ Nanoparticles؛ DRX
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